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The organic phase was dried over anhydrous MgSO 4 and, after evaporation of the solvent under reduced pressure, the totally protected dipeptide 1 was purified on a silica gel column in AcOEt/cyclohexane, 7:3, as the eluent
This is the same freeze-drying process used across pharmaceutical manufacturing to extend the stability of sensitive peptide compounds
However, control of the mechanism of GSH synthesis in malignant tumors remains poorly understood
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